A new process for extraction of titanium metal from its oxide is demonstrated.
In this process, row material to be reduced is titanium oxide synthesized from
ilmenite. The reducing agent is the Ca+CaCl2 two-phase mixture. Titanium is
elaborated in the medium consisted of liquid Ca, CaCl2 and solid TiO2 at
the temperature range 1200 to 1300K by means of mixing mechanically the
ingredients in the reactor into a smooth paste. Fluidity of the feed which
enables continuous scheme depends on the CaCl2 content. The oxygen level of
the reduced titanium is the range 500 to 1000 mass ppm varying with the
operational conditions. The Ca+CaCl2 reducing agent is taken out from the
electrolysis of CaCl2 at 1140K, and this CaCl2 is produced by aqueous
chemistry conversion using Cl2 gas recycled from the electrolysis.