Journal of Physical Chemistry, B, 110(34) 16808-16811(2006〕

Direct Detection of OH Radicals Diffused to the Gas Phase from the UV-irradiated Photocatalytic TiO2 Surfaces by means of Laser-Induced Fluorescence Spectroscopy.

Yoshinori Murakami,* Endo Kenji, Atsuko Y Nosaka, and Yoshio Nosaka*

Abstract
The important roles of OH radicals for remote oxidation using TiO2 photocatalysts were evidenced by the in situ detection of OH radicals in the gas phase using the laser-induced fluorescence (LIF) technique. The appearance of OD-LIF intensities after the exposure of D2O vapors over TiO2 powders and the decrease of the time-resolved signals of OH-LIF intensities with increasing calcined temperatures of TiO2 powders suggested that the exchangeable water at the TiO2 surface is the origin of the diffused OH radicals.

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